It would be ideal if I could decompose it to sodium chloride. It is a white crystalline, hygroscopic solid that is highly soluble in water and in alcohol. SAFETY DATA SHEET: SODIUM PERCHLORATE, Monohydrate SODIUM PERCHLORATE, Monohydrate S512.10 INTEGRA Chemical Company 24 Hour Emergency Response: CHEMTREC 800-424-9300 (Outside USA 703-527-3887) 1216 6th Ave N Kent WA 98032 This process is the main outlet for the industrial production of perchloric acid. Sodium perchlorate is the inorganic compound with the chemical formula NaClO4. The commercial ammonium perchlorate product is manufactured by the double-exchange reaction of sodium perchlorate and ammonium chloride. The salt also can be produced by salt metathesis reaction of ammonium salts with sodium perchlorate. Perchlorate is usually found as the anion component of a salt most often associated with cations such as ammonium, sodium, or potassium. Disposal /decomposition of sodium perchlorate. Potassium perchlorate is more stable.
It usually encountered as the monohydrate. The best bet is to make sodium perchlorate and then potassium perchlorate.

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The only sensible and feasable way to purify Sodium Perchlorate from Chlorate contamination is to destroy all traces of Chlorate by chemical treatement. Potassium Perchlorate is the potassium salt of perchloric acid and a member of the Hofmeister ions series with thyroid blocking properties. MSDS Name: Sodium perchlorate monohydrate Catalog Numbers: AC343630000, AC343630010, AC343631000, S360-212, S360-500, S490-100, S490-500 Synonyms: Perchloric acid, sodium salt, monohydrate. It is typically found in the form of perchloric acid and salts such as ammonium perchlorate, potassium perchlorate, and sodium perchlorate. The compound is noteworthy as the most water-soluble of the common perchlorate salts. Company Identification: Fisher Scientific 1 Reagent Lane Fair Lawn, NJ 07410 Soidum perchlorate is made by continuing the electrolysis process for a longer time. I have access to a fair number of reagents.
NaCIO3 + KCl -> KClO4 + NaCl (5) Either the purified sodium perchlorate cell solution or sodium perchlorate crystals dissolved in water is treated with potassium chloride. After about 156 hours of electolysis the oringinal sodium chloride solution will become sodium perchlorate … What is the safest way to dispose of a solution of sodium perchlorate? Destroying Chlorate with chemicals When making Perchlorates from Sodium Perchlorate you must have pure Perchlorate. Ammonium perchlorate (AP) is produced by reaction between ammonia and perchloric acid. Please try again later. Potassium perchlorate is prepared by the double decomposition reaction of sodium perchlorate and potassium chloride. Potassium perchlorate is prepared industrially by treating an aqueous solution of sodium perchlorate with potassium chloride.This single precipitation reaction exploits the low solubility of KClO 4, which is about 1/100 as much as the solubility of NaClO 4 (209.6 g/100 mL at 25 °C).. I either need to make it safe to dump down a drain or put it in a hazmat drum. Ammonia , hydrochloric acid , and sodium perchlorate are mixed and the reaction mixture crystallized in a vacuum-cooled crystallizer.